切换至 "中华医学电子期刊资源库"

中华口腔医学研究杂志(电子版) ›› 2011, Vol. 5 ›› Issue (06) : 577 -583. doi: 10.3877/cma.j.issn.1674-1366.2011.06.004

基础研究

不同包埋材料对铸造纯钛铸件表面硬化层的影响
梁钦业1,(), 吴夏怡1   
  1. 1.510055 广州,中山大学光华口腔医学院·附属口腔医院·口腔医学研究所
  • 收稿日期:2011-07-12 出版日期:2011-12-01
  • 通信作者: 梁钦业

The surface hardness layer analysis of the titanium casting manufactured by two different titanium casting investment material

Qin-ye LIANG1,(), Xia-yi WU1   

  1. 1.Guanghua School of Stomatology, Institute of Stomatological Research, Sun Yat-sen University, Guangzhou 510055,China
  • Received:2011-07-12 Published:2011-12-01
  • Corresponding author: Qin-ye LIANG
引用本文:

梁钦业, 吴夏怡. 不同包埋材料对铸造纯钛铸件表面硬化层的影响[J/OL]. 中华口腔医学研究杂志(电子版), 2011, 5(06): 577-583.

Qin-ye LIANG, Xia-yi WU. The surface hardness layer analysis of the titanium casting manufactured by two different titanium casting investment material[J/OL]. Chinese Journal of Stomatological Research(Electronic Edition), 2011, 5(06): 577-583.

目的

研究两种不同包埋材料对铸件表面硬化层的影响。

方法

用铸造蜡片制作尺寸为20 mm×20 mm×1.5 mm 的片状试件共6 片,分为2 组,实验组采用新型铸钛包埋材料包埋,对照组采用Rematitan Plus 专用铸钛包埋料包埋铸造。 铸件处理后用显微硬度仪测试表面硬度,负重200 g 持续5 s,测量维氏显微硬度值,比较不同铸钛包埋材料所铸的铸件表面显微硬度,从而判断包埋料对铸件表面硬化层的影响。

结果

实验组纯钛铸件表面的维氏显微硬度值较高,为(255.33±16.042) HV;随着测量位点与表面距离增加,维氏显微硬度值降低,纯钛铸件表面的硬化层厚度约50 μm。 对照组纯钛铸件表面的维氏显微硬度升高显著,为(416.33±6.506) HV;随着测量位点与表面距离增加,维氏显微硬度值逐渐降低,但硬化层较厚,约140 μm。

结论

用新型铸钛包埋材料所铸的纯钛铸件表面的硬化层厚度较低,对铸件的理化性能影响较小,能满足精密铸造修复体的应用要求。

Objective

To investigate the micro-hardness of the titanium castings manufactured by a new investment for titanium casting.

Methods

Six titanium casting specimens(20 mm × 20 mm × 1.5 mm) were divided into two groups and cast by a new titanium investment material and Rematitan Plus investment material, respectively.Micro-hardness was measured by a micro-hardness instrument (Leitz Wetzlar, Germany) under a load of 200 g for 5 s at different points from the surface to the interior on sections of specimens embedded in acrylic resin.The thickness of the micro-hardness layers of the two titanium castings was compared.

Results

Vicker's hardness of the tested specimens was higher at the surface layers than in the inner layers.However, the increasing rate of the hardness at the surface layer is smaller with the new titanium investments than with Rematitan Plus investments.The micro-hardness layer of the titanium casting manufactured by the new titanium investments is 50 μm through the cross-section of the surface, thinner than that of Rematitan Plus' (140 μm).

Conclusions

The new titanium investments were more suitable for titanium casting than the Rematitan Plus investments.Titanium castings, such as crowns, removable partial denture frame-works, could be manufactured successfully by the new titanium investments.

图1 片状蜡型试件铸道安插示意图
表1 新型铸钛包埋材料所铸纯钛铸件断面维氏显微硬度值的(±s,HV)
表2 新型包埋材料组数据单因素方差分析(ANOVA)结果
表3 新型包埋材料组数据比较结果
表4 Rematitan Plus 专用铸钛用包埋材料所铸纯钛铸件断面的维氏显微硬度值(±s,HV)
表5 对照组共7 组数据单因素方差分析(ANOVA)结果
表6 对照组数据比较结果
图2 不同包埋材料对纯钛铸件表面维氏显微硬度的影响
1
杨道明,朱勋,李紫桐.金属力学性能与失效分析.北京:冶金工业出版社, 1991:85-88.
2
Chai TI, Stein RS.Porosity and accuracy of multiple-unit titanium castings.J Prosthet Dent.1995,73(6):534-541.
3
汪大林.钛在口腔医学中的应用研究.国外医学·口腔医学分册, 1993,20(1):43-46.
4
宫相芹,冯悦慧,田立坤,等.不同比例ZrP99 包埋材料对钛铸件质量影响的实验研究.辽宁医学杂志, 2002,16(2):67-69.
5
Mori T, Jean-Louis M, Yabugami M, et al.The effect of investment type on the fit of cast titanium crowns.Aust Dent J, 1994,39(6):348-352.
6
Ida K, Takeuchi M, Togaya T, et al.Studies on the dental casting of titanium alloy (Part 1.Casting of pure titanium).J Jpn Res Soc Dent Mater Appl, 1980,37:45-52.
7
Ida K, Togaya T, Tsutsumi S, et al.Effect of magnesia investments in the dental casting of pure titanium or titanium alloys.Dent Mater J,1982,1(1):8-21.
8
Luo XP, Guo TW, Ou YG, et al.Titanium casting into Phosphate bonded investment with zirconite.Dent Mater, 2002,18(7):512-515.
9
Miyakawa O, Watanabe K, Okawa S, et al.Layered structure of cast titanium surface.Dent Mater J, 1989,8(2):175-185.
10
梁钦业,赵云凤,肖茂春.新型铸钛包埋材料不同铸模温度对纯钛铸流率影响的研究[J/CD].中华口腔医学研究杂志:电子版, 2009,3(1):59-65.
[1] 苏育武, 支清惠, 崔添强, 刘姗姗, 郑军, 林焕彩. 树脂浸润对人工龋表面硬度及变异链球菌生物膜形成的影响[J/OL]. 中华口腔医学研究杂志(电子版), 2016, 10(05): 303-308.
[2] 许嘉允, 邓飞龙, 庄秀妹, 欧阳江林, 刘芸, 王婧, 李夏晨. 纯钛微纳米复合形貌对成骨细胞生物学行为的影响[J/OL]. 中华口腔医学研究杂志(电子版), 2015, 09(06): 461-469.
[3] 李小龙, 覃峰, 钱宇, 尹映竹, 黄雪清, 罗涛. 改良自酸蚀粘接剂对龋影响牙本质粘接性能的影响[J/OL]. 中华口腔医学研究杂志(电子版), 2015, 09(04): 295-300.
[4] 何华伟, 郑东翔. 义齿基托材质与患者初戴满意度及咀嚼效率的关系[J/OL]. 中华口腔医学研究杂志(电子版), 2015, 09(03): 200-204.
[5] 张艺萍, 叶剑涛. 表面处理技术提高钛-瓷结合强度的研究进展[J/OL]. 中华口腔医学研究杂志(电子版), 2012, 6(04): 382-385.
[6] 于春梅, 王洋, 李瑞虹. 照射时间及温度对纳米树脂硬度的影响[J/OL]. 中华口腔医学研究杂志(电子版), 2011, 5(04): 387-391.
[7] 王萍, 林焕彩. 唾液对牙釉质酸蚀保护作用的体外实验研究[J/OL]. 中华口腔医学研究杂志(电子版), 2011, 5(01): 19-25.
阅读次数
全文


摘要